Analytical Profiles of Drug Substances, Vol. 1 by FLOREY KLAUS

By FLOREY KLAUS

Profiles of Drug ingredients, Excipients and comparable method vol 1. content material: entrance hide; Analytical Profiles of Drug components, quantity 1; Copyright web page; Contents; AFFILIATIONS OF EDITORS, participants, AND REVIEWERS; FOREWORD; PREFACE; bankruptcy 1. Acetohexamide; bankruptcy 2. Chlordiazepoxide; bankruptcy three. Chlordiazepoxide Hydrochloride; bankruptcy four. Cycloserine; bankruptcy five. Cyclothiazide; bankruptcy 6. Diazepam; bankruptcy 7. Erythromycin Estolate; bankruptcy eight. Halothane; bankruptcy nine. Levarterenol Bitartrate; bankruptcy 10. Meperidine Hydrochloride; bankruptcy eleven. Meprobamate; bankruptcy 12. Nortriptyline Hydrochloride; bankruptcy thirteen. Potassium Phenoxymethyl Penicillin. bankruptcy 14. Propoxyphene HydrochlorideChapter 15. Sodium Cephalothin; bankruptcy sixteen. Sodium Secobarbital; bankruptcy 17. Triamcinolone; bankruptcy 18. Triamcinolone Acetonide; bankruptcy 19. Triamcinolone Diacetate; bankruptcy 20. Vinblastine Sulfate; bankruptcy 21. Vincristine Sulfate. summary: Profiles of Drug components, Excipients and comparable method vol 1

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2,0, 2,s 40 30 :20 10 I , , , , . , I , I , , , , . . , 4000 3800 3400 3000 2600 2200 1900 1700 1600 1300 WAVENUMBER C M . l F i g . 1. , . ll00 . 900 . 700 . 0 Fig. 2. 0 1 0 Nuclear magnetic r e s o n a n c e c y c l o s e r i n e 56 1 300 CYCLOSE R IN€ tively. 68 ppm a r e t h e t h r e e m a g . : c t i c a l l y nonequivalent isoxazolidone r i n g protcps. 111 H C 1 3 . 6 D i f f e r e n t i a l Thermal A n a l y s i s X d i f f e r e n t i a l t h e r m a l a n a l y s i s ivas p e r f o r a e d on c y c l o s e r i n e .

The exotherm observed a t 233°C c o r r e s p o n d s t o t h e m e l t i n g of t h e d r u g f o l l o w e d by decomp o s i t i o n a t a p p r o x i m a t e l y 241OC. 5 kcal/mole8. 8 Thermogravimetric A n a l y s i s A TGA scan performed on c h l o r d i a z e p o x i d e hydroc h l o r i d e e x h i b i t e d 90 l o s s of w e i g h t when h e a t e d t o 1O5OC8. 10 Crystal Properties The x-ray powder d i f f r a c t i o n p a t t e r n of c h l o r d i a z e p o x i d e h y d r o c h l o r i d e is p r e s e n t e d i n T a b l e 111'.

A. , J . Pharm. S c i . , 2, 1569 (1970). A. , and D'Arconte, L. , Anal. , 5, 195 (1963). A. , Krol, G. , J . PharmacoZ. Exp. , 148, 339 (1965). , J. Pharm. S c i . , 55, 1358 (1966). , Personal Communication. 36 CHLORDIAZEPOXI DE 21. 22. 23. 24. 25. 26. National FomuZary XIII, 148-149 ( 1 9 7 0 ) . R o e t e r , E. , Z e i t , f. Anal. , (1969). D. 18, 529 ( 1 9 6 8 ) . , E , 45 and S m i t h , S . J . , Arneim. , Tomoda, M. Kyoritsu Yakka Daigaku Kenkyv Neppo, 18 ( 1 9 6 5 ) . Thomas, J . J .

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